반응 #651856

ord-32133b7696f84760b3d9b3bd7d4f8855

반응 방정식

CCCCCCOc1ccc2c(c1)CC(O)c1cc(OCCCCCC)ccc1-2
2,7-dihexyloxy-9,10-dihydrophenanthren-9-ol
CCN(CC)S(F)(F)F
DAST
→
CCCCCCOc1ccc2c(c1)CC(F)c1cc(OCCCCCC)ccc1-2
9-Fluoro-2,7-dihexyloxy-9,10-dihydrophenanthrene

반응물

CCCCCCOc1ccc2c(c1)CC(O)c1cc(OCCCCCC)ccc1-2
2,7-dihexyloxy-9,10-dihydrophenanthren-9-ol
CCN(CC)S(F)(F)F
DAST

시약

없음

용매

ClCCl
dichloromethane

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

From 2,7-dihexyloxy-9,10-dihydrophenanthren-9-ol by reaction with DAST in abs. dichloromethane.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06168838Auspto-grants-2001_01