반응 #65101

반응 방정식

4-n-octyloxyterphenyl-4"-carboxylic acid

thionyl chloride

→

4-n-octyloxyterphenyl-4"-carboxylic acid chloride

반응 조건

후처리

1. 1
   온도under reflux condition for 6 hours
2. 2
   workup.DISTILLATIONunreacted thionyl chloride was distilled off

실험 절차

After 1.6 g of 4-n-octyloxyterphenyl-4"-carboxylic acid was heated with an excess amount of thionyl chloride under reflux condition for 6 hours, unreacted thionyl chloride was distilled off to obtain 4-n-octyloxyterphenyl-4"-carboxylic acid chloride.

출처