반응 #64954

반응 방정식

6-benzyl-1-methyl-octahydropyrrolo[3,4-b]pyridine

dihydrochloride

→

1-Methyl-octahydropyrrolo[3,4-b]pyridine

용매

methanol

반응 조건

후처리

1. 1
   workup.DISTILLATIONWorking up by distillation
2. 2
   기타gives 2.6 g (34% of theory) of a colorless oil of boiling point 83°-85°/12 mbar)

실험 절차

11.7 g (54 retool) of 6-benzyl-1-methyl-octahydropyrrolo[3,4-b]pyridine as the dihydrochloride are hydrogenated in 100 ml of methanol over palladium-on-active charcoal in accordance with the working instructions of Example Id. Working up by distillation gives 2.6 g (34% of theory) of a colorless oil of boiling point 83°-85°/12 mbar).

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