반응 #64949

반응 방정식

6-benzyl-5,7-dioxo-octahydropyrrolo[3,4-b ]pyridine

lithium aluminum hydride

→

6-Benzyl-octahydropyrrolo[3,4-b]pyridine

용매

tetrahydrofuran

반응 조건

후처리

1. 1
   기타are obtained on distillation

실험 절차

44 g (about 0.18 mol) of crude or pure 6-benzyl-5,7-dioxo-octahydropyrrolo[3,4-b ]pyridine are reduced with 15.2 g (0.40 mol ) of lithium aluminum hydride in 390 ml of absolute tetrahydrofuran in the course of 10 hours in accordance with the working instructions of Example Ic. 4.4 g of a colorless oil having a boiling point of 93°-95° C./0.06 mbar are obtained on distillation.

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