반응 #648888

ord-154f3c784501405e9b764ffb2d623369

반응 조건

온도
80°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타1.31 g (56% of theory) of the target compound were obtained

실험 절차

The title compound was prepared starting from 1.00 g (5.64 mmol) of the compound from Example 8A and 1.41 g (5.64 mmol) of the compound from Example 182A in analogy to the synthesis of the compound from Example 278. A difference was that stirring at 80° C. was for only 4 h. 1.31 g (56% of theory) of the target compound were obtained.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08063234B2uspto-grants-2011_11