반응 #64702

반응 방정식

1-ethylpiperidine

formic acid

Meldrum's acid

veratraldehyde

→

3-(3,4-dimethoxyphenyl)propionic acid

반응 조건

후처리

1. 1
   기타reacted at the same temperature for 2 hours

실험 절차

After dropwise adding 27.2 g (33.1 ml, 0.24 mol) of 1-ethylpiperidine to 27.6 g (22.6 ml, 0.6 mol) of formic acid under stirring, 7.2 g (0.05 mol) of Meldrum's acid and 8.3 g (0.05 mol) of veratraldehyde were added to the solution which was then heated to 95° C. during 1 hour and reacted at the same temperature for 2 hours. Subsequently the method of Example 1 was followed.

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