반응 #64698
ord-34d196c1fab248819f8d6892c2587e9f
반응 조건
온도
105°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타prepared
- 2기타reacted at the same temperature for 1 hour
- 3기타The product was isolated
실험 절차
3.60 g (0.025 mol) of Meldrum's acid and 3.8 g (0.025 mol) of p-nitrobenzaldehyde were weighed in to 25 ml of the mixture of formic acid and triethylamine prepared as described in Example l. The reaction mixture was heated to 105° C. during 1 hour and reacted at the same temperature for 1 hour. The product was isolated according to Example 1.