반응 #64694
ord-7ed3b08e75fa49089858a61a38270641
반응 조건
온도
95°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타prepared
- 2온도maintained at the same temperature for 2 hours
- 3기타The product was separated
실험 절차
7.2 g (0.05 mol) of Meldrum's acid and 6.6 g (6.3 ml, 0.05 mol) of cinnamaldehyde were weighed in to 50 ml of the mixture of formic acid and triethylamine prepared as described in Example 1. The reaction mixture was heated to 95° C. during 1 hour and maintained at the same temperature for 2 hours. The product was separated according to Example 1.