반응 #64243

ord-99a05bba987e495ba5a0d1f076287117

반응 방정식

CCN(C(C)=O)[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-ethyl-N-acetyl-4-nitroxycyclohexylamine
CCN[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-ethyl-4-nitroxycyclohexylamine
→
CC(=O)N[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-acetyl-4-nitroxycyclohexylamine
수율 35.0%

반응물

CCN(C(C)=O)[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-ethyl-N-acetyl-4-nitroxycyclohexylamine
CCN[C@H]1CC[C@H](O[N+](=O)[O-])CC1
trans-N-ethyl-4-nitroxycyclohexylamine

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

trans-N-ethyl-N-acetyl-4-nitroxycyclohexylamine from trans-N-ethyl-4-nitroxycyclohexylamine melting point: 68°-69° C. (ether), yield: 35% of theory.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05411989uspto-grants-1995_05