반응 #64238

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4-benzyloxycarbonylbenzoic acid

N,N-diethylethylene diamine

→

4-([2-(N,N-diethylamino)ethyl]aminocarbonyl)benzoic acid

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실험 절차

4-([2-(N,N-diethylamino)ethyl]aminocarbonyl)benzoic acid was prepared from 4-benzyloxycarbonylbenzoic acid by reaction with N,N-diethylethylene diamine to yield the mono amide derivative which was hydrogenolysed to give the acid (CI-MS: m/z 265 [M+b]+).

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