반응 #64223

반응 방정식

acetone cyanohydrin

4-amino 1-butanol

→

propanonitrile

2-(4-hydroxybutylamino) 2-methylpropano-nitrile

용매

methylene chloride

반응 조건

후처리

1. 1
   기타dried
2. 2
   여과filtered
3. 3
   농축the filtrate was concentrated under reduced pressure

실험 절차

220 μl of acetone cyanohydrin and 200 μl of 4-amino 1-butanol were mixed together with stirring for 16 hours at 20° C. and then was diluted with 2 ml of methylene chloride, dried, filtered and the filtrate was concentrated under reduced pressure to obtain the propanonitrile which was used as is for the following stage.

출처