반응 #64221

반응 방정식

methylene chloride

acetone

ethyl acetate

product

4-(4,4-dimethyl 3-(4-hydroxybutyl)-5-imino 2-thioxo 1-imidazolidinyl) 2-(trifluoromethyl) benzonitrile

→

expected product

4-(4,4-dimethyl 3-(4-hydroxybutyl)-5-oxo 2-thioxo-1-imidazolidinyl) 2-(trifluoromethyl) benzonitile

반응 조건

후처리

1. 1
   기타were reacted

실험 절차

Using the procedure of Example 71, 300 mg of the product of Example 76 were reacted to obtain 236 mg of the expected product melting at 78°-79° C. with a Rf=0.31 (eluant: methylene chloride--acetone (75-25)).

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