반응 #640568
ord-357c4cbcd5cd4528851205250f3de92c
반응 방정식
diethyl ether
Phenacyl bromide
tetrahydrothiophene
water
→
Phenacyltetrahydrothiophenium Bromide
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The aqueous layer separated
실험 절차
Phenacyl bromide, 88.2 g (0.44 mole) and tetrahydrothiophene, 39.1 g (0.44 mole) were dissolved in 220 g of nitromethane, which was stirred for 4 hours at room temperature. The reaction solution was combined with 800 g of water and 400 g of diethyl ether. The aqueous layer separated was taken out, which was an aqueous solution of the target compound, phenacyltetrahydrothiophenium bromide.