반응 #640563

반응 방정식

2-aminophenylboronic acid

acryloyl chloride

→

2-Acrylamido-phenylboronic acid

반응 조건

후처리

1. 1
   추출The product was extracted in acetone
2. 2
   기타dried
3. 3
   기타a rotary evaporator

실험 절차

2-Acrylamido-phenylboronic acid (“2-APB”) was synthesized by reacting 2-aminophenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 2-APB was confirmed using NMR. The purity was shown to be greater than 90%.

출처