반응 #640562

반응 방정식

3-amino phenylboronic acid

acryloyl chloride

→

3-Acrylamido-phenylboronic acid

반응 조건

후처리

1. 1
   추출The product was extracted in acetone
2. 2
   기타dried
3. 3
   기타a rotary evaporator

실험 절차

3-Acrylamido-phenylboronic acid (“3-APB”) was synthesized by reacting 3-amino phenylboronic acid with an excess of acryloyl chloride in an aqueous alkaline solution. The product was extracted in acetone and dried using a rotary evaporator. The structure of 3-APB was confirmed using NMR. The purity was about 90%, TLC showing very little contamination.

출처