반응 #640553

반응 방정식

Hexyltrimethylammonium hydroxide

tetraethylorthosilicate

→

Hexyltrimethylammonium Silicate

용매

water

반응 조건

후처리

1. 1
   기타After hydrolysis
2. 2
   기타the solution was placed on a rotary evaporator
3. 3
   기타to remove the alcohol
4. 4
   기타A total of 518.6 g of liquid was removed
5. 5
   workup.ADDITIONafter which 150 g of deionized water was added

실험 절차

Hexyltrimethylammonium hydroxide, (30.03%), 492.96 g, was diluted with 1073.86 g deionized water and to it there were added 650.0 g of tetraethylorthosilicate, (98%) with stirring. After hydrolysis was complete, the solution was placed on a rotary evaporator to remove the alcohol. A total of 518.6 g of liquid was removed, after which 150 g of deionized water was added. Elemental analysis showed the solution to contain 5.10 wt % Si.

출처