반응 #63786

ord-c6297e97bed54076a52d42942f386a2e

반응 방정식

O=[N+]([O-])[O-].[Ag+]
silver nitrate
c1ccc2[nH]nnc2c1
benzotriazole
[Ag].c1ccc2[nH]nnc2c1
silver benzotriazole

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타was kept at 40° C.
  2. 2
    기타removed from the resulting emulsion by pH-adjustment

실험 절차

In 3,000 ml of water were dissolved 28 g of gelatin and 13.2 g of benzotriazole, and the solution was kept at 40° C. while stirring. To the solution was added 100 ml of an aqueous solution of 17 g of silver nitrate over 2 minutes. Excessive salts were sedimented and removed from the resulting emulsion by pH-adjustment. Thereafter, the emulsion was adjusted to pH 6.50 to obtain a silver benzotriazole emulsion. The yield of the emulsion was 400 g.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04767690uspto-grants-1988_08