반응 #63786
ord-c6297e97bed54076a52d42942f386a2e
반응 방정식
silver nitrate
benzotriazole
→
silver benzotriazole
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타was kept at 40° C.
- 2기타removed from the resulting emulsion by pH-adjustment
실험 절차
In 3,000 ml of water were dissolved 28 g of gelatin and 13.2 g of benzotriazole, and the solution was kept at 40° C. while stirring. To the solution was added 100 ml of an aqueous solution of 17 g of silver nitrate over 2 minutes. Excessive salts were sedimented and removed from the resulting emulsion by pH-adjustment. Thereafter, the emulsion was adjusted to pH 6.50 to obtain a silver benzotriazole emulsion. The yield of the emulsion was 400 g.