반응 #6371

반응 방정식

γ-chloropropyltrimethoxysilane

potassium acrylate

→

γ-acryloxypropyltrimethoxysilane

반응 조건

후처리

1. 1
   기타followed by removal of potassium chloride
2. 2
   workup.DISTILLATIONwere distilled off under reduced pressure

실험 절차

Trichlorosilane and allyl chloride were subjected to hydrosilylation reaction in a solvent in the presence of a platinum catalyst, followed by esterification reaction with methanol and urea and further by distillation to obtain γ-chloropropyltrimethoxysilane. The thus obtained γ-chloropropyltrimethoxysilane and potassium acrylate were subjected to desalting in a solvent, followed by removal of potassium chloride. Subsequently, low boiling components including the solvent were distilled off under reduced pressure to obtain crude γ-acryloxypropyltrimethoxysilane having a purity of approximately 90%.

출처