반응 #63456

반응 방정식

3,4-Dihydro-3-oxo-1,4(2H)-benzoxazine

diborane

sodium hydroxide

→

title compound

3,4-Dihydro-1,4(2H)-benzoxazine

용매

tetrahydrofuran

반응 조건

후처리

1. 1
   추출the product was extracted with ether
2. 2
   기타the solvent was evaporated

실험 절차

3,4-Dihydro-3-oxo-1,4(2H)-benzoxazine was refluxed for several hours in one equivalent of diborane in tetrahydrofuran. Excess sodium hydroxide solution was added, the product was extracted with ether and the solvent was evaporated to give the title compound as an oil.

출처