반응 #63443

ord-ea00ba65867849b59ddc89beb0e3ca9d

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and 2-butanol there is obtained 2-butyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a resinous product, 1H-NMR(CDCl3): 1.02 (t, CH2CH3), 1.35 (d, CH--CH3), 1.4-2.0 (m, 2H), 4.23 (s, 4H), 4.83 (m, 1H), 7.3-7.7 (8H);

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04766115uspto-grants-1988_08