반응 #63354

ord-e662789599884e72a40dfc84bcd03121

반응 방정식

CCCCCC
hexane
C=C(C(=O)O)c1ccc([N+](=O)[O-])cc1
a-(4-nitrophenyl)-acrylic acid
O=C(Cl)C(=O)Cl
oxalyl chloride
C=CC(=O)NC1CCCCC1
N-cyclohexylacrylamide
→
C=CC(=O)C(C(=O)C(=C)c1ccc([N+](=O)[O-])cc1)C1CCNCC1
title compound
C=CC(=O)C(C(=O)C(=C)c1ccc([N+](=O)[O-])cc1)C1CCNCC1
4-aza-4-cyclohexyl-2-(4-nitrophenyl)-1,6-heptadiene-3,5-dione

반응물

CCCCCC
hexane
C=C(C(=O)O)c1ccc([N+](=O)[O-])cc1
a-(4-nitrophenyl)-acrylic acid
O=C(Cl)C(=O)Cl
oxalyl chloride
C=CC(=O)NC1CCCCC1
N-cyclohexylacrylamide

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The title compound is prepared analogously to Example 1c starting from 40.5 g of a-(4-nitrophenyl)-acrylic acid, 26.7 g of oxalyl chloride and 26.8 g of N-cyclohexylacrylamide. Melting point 73°-74° (from hexane).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04764640uspto-grants-1988_08