반응 #63349

반응 방정식

3-methyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.1]heptane-2,4-dione

ethyl acetate

→

1-(4-aminophenyl)-3-methyl-3-azabicyclo[3.1.1]heptane-2,4-dione

용매

2-methoxyethanol

반응 조건

실험 절차

In a manner analogous to that described in Example 1a, 6.0 g of 3-methyl-1-(4-nitrophenyl)-3-azabicyclo[3.1.1]heptane-2,4-dione are dissolved in 120 ml of 2-methoxyethanol, hydrogenated in the presence of 0.6 g of 5% palladium-on-carbon and worked up. Melting point 197°-198° (from ethyl acetate)

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