반응 #63312

반응 방정식

cyanocarbonimidodithioic acid dimethyl ester

benzaldehyde N-methyl hydrazone

→

title compound

N-Cyano-1-methyl-2-(phenylmethylene)hydrazinecarboximidothioic acid, methyl ester

용매

acetonitrile

반응 조건

후처리

1. 1
   온도was heated
2. 2
   온도under reflux for 50 hr
3. 3
   온도The reaction mixture was cooled to 25°

실험 절차

A mixture of cyanocarbonimidodithioic acid dimethyl ester (1.46 g) and benzaldehyde N-methyl hydrazone (1.34 g) in acetonitrile was heated under reflux for 50 hr. The reaction mixture was cooled to 25° to give the title compound as colourless crystals, m.p. 132°-133° (0.73 g).

출처