반응 #63291

반응 방정식

iodobenzene

diphenylamine

potassium hydroxide

→

triphenylamine

수율 82.0%

반응 조건

후처리

1. 1
   workup.ADDITIONfollowing charge
2. 2
   기타The above-identified product was obtained as colorless crystals

실험 절차

The same equipment and conditions as in example I were employed with the following charge: 20.4 grams (0.1 mole) iodobenzene, 27.4 grams (0.15 mole) diphenylamine, 16.8 grams (0.3 mole) potassium hydroxide flakes, 15.0 grams of copper powder and 30.0 milliliters of Soltrol® 170. The above-identified product was obtained as colorless crystals having a melting point of 125°-126° C. Yield 82%.

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