반응 #632008

반응 방정식

ethyl acetate

N-tert-butyl-(1-methyl)cyclopropylsulfonamide

benzyl bromide

→

desired product

수율 60.0%

N-tert-butyl-(1-benzyl)cyclopropyl-sulfonamide

수율 60.0%

용매

hexane

반응 조건

후처리

1. 1
   기타This compound was obtained in 60% yield

실험 절차

This compound was obtained in 60% yield using the procedure described for the synthesis of N-tert-butyl-(1-methyl)cyclopropylsulfonamide using 1.05 equivalents of benzyl bromide. Trituration with 10% ethyl acetate in hexane provided the desired product: 1H NMR (CDCl3) δ 0.92 (m, 2H), 1.36 (m, 2H), 1.43 (s, 9H), 3.25 (s, 2H), 4.62 (br s, 1H), 7.29-7.36 (m, 5H).

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