반응 #631975
ord-55cefff41d0346b1bd2437b3200c3d54
반응 방정식
6-hydroxy-2-naphthyl benzoate
nitric acid
water
→
6-hydroxy-5-nitro-2-naphthyl benzoate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타at 15° C.
- 2기타The thus obtained deposit was recrystallized from ethanol/acetic acid
실험 절차
The thus obtained 6-hydroxy-2-naphthyl benzoate was dispersed in acetic acid, nitric acid was added dropwise to the dispersion while keeping it at 15° C., and water was further added thereto, followed by stirring. The thus obtained deposit was recrystallized from ethanol/acetic acid to obtain 6-hydroxy-5-nitro-2-naphthyl benzoate.