반응 #631971

반응 방정식

2-Carboxyethyl acrylate

Thionyl chloride

→

desired product

3-chloro-3-oxopropyl acrylate

용매

CH2Cl2

반응 조건

후처리

1. 1
   온도the solution is cooled in an ice bath
2. 2
   기타The solvent is removed under reduced pressure

실험 절차

2-Carboxyethyl acrylate (1 eq.) is dissolved in CH2Cl2 and the solution is cooled in an ice bath. Thionyl chloride (1 eq.) is added dropwise and the mixture is allowed to warm to room temperature and stir for 4 hours. The solvent is removed under reduced pressure and the desired product is isolated by vacuum distillation.

출처