반응 #63172
ord-86168dd4db814de98319e1b2cb3e7425
반응 방정식
benzotriazole
silver nitrate
→
silver benzotriazole
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타was kept at 40° C.
- 2기타removed from the resulting emulsion by pH adjustment
실험 절차
In 3,000 ml of water were dissolved 28 g of gelatin and 13.2 g of benzotriazole, and the solution was kept at 40° C. while stirring. To the solution was added 100 ml of an aqueous solution containing 17 g of silver nitrate over 2 minutes. Excess salts were sedimented and removed from the resulting emulsion by pH adjustment. Thereafter, the emulsion was adjusted to a pH of 6.30 to obtain a silver benzotriazole emulsion. The yield of the emulsion was 400 g.