반응 #63172

ord-86168dd4db814de98319e1b2cb3e7425

반응 방정식

c1ccc2[nH]nnc2c1
benzotriazole
O=[N+]([O-])[O-].[Ag+]
silver nitrate
[Ag].c1ccc2[nH]nnc2c1
silver benzotriazole

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타was kept at 40° C.
  2. 2
    기타removed from the resulting emulsion by pH adjustment

실험 절차

In 3,000 ml of water were dissolved 28 g of gelatin and 13.2 g of benzotriazole, and the solution was kept at 40° C. while stirring. To the solution was added 100 ml of an aqueous solution containing 17 g of silver nitrate over 2 minutes. Excess salts were sedimented and removed from the resulting emulsion by pH adjustment. Thereafter, the emulsion was adjusted to a pH of 6.30 to obtain a silver benzotriazole emulsion. The yield of the emulsion was 400 g.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04764451uspto-grants-1988_08