반응 #62970

반응 방정식

bromomethyl ethylene glycol

magnesium sulfate

acetone

→

crude product

2,2-Dimethyl-4-bromomethyl-1,3-dioxolane

반응 조건

후처리

1. 1
   기타The cooled reaction mixture
2. 2
   여과is filtered
3. 3
   기타the solvent is removed

실험 절차

An acetone solution of bromomethyl ethylene glycol is refluxed for 24 hours in the presence of anhydrous magnesium sulfate. The cooled reaction mixture is filtered and the solvent is removed to provide a residual crude product.

출처