반응 #626150

ord-17d89f5f75154560a35f326706e8dd50

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타is prepared

실험 절차

Furthermore, as a method for producing bis(aminomethyl)cyclohexane, for example, Non-Patent Document 1 (Malachowski et al.) discloses the following: an acid chloride derivative is prepared using cyclohexanedicarboxylic acid with thionyl chloride; cyclohexane diamide is prepared using the acid chloride derivative with ammonia; and thereafter, the cyclohexane diamide is further allowed to react with thionyl chloride to obtain dicyanocyclohexane, and then the obtained dicyanocyclohexane is hydrogenated.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08865938B2uspto-grants-2014_10