반응 #62390

반응 방정식

methyl hydrazine

di-tert-butyldicarbonate

→

title compound

N-Methyl-hydrazine carboxylic acid tert-butyl ester

용매

ethanol

ethanol

반응 조건

후처리

1. 1
   온도cooling
2. 2
   workup.STIRRINGAfter stirring at room temperature for 7 hours
3. 3
   기타the solvent was evaporated

실험 절차

10 mL of methyl hydrazine was dissolved in 90 mL of ethanol, and under stirring at ice-cooling, a solution of 41 g of di-tert-butyldicarbonate in 90 mL of ethanol was added dropwise over 45 minutes. After stirring at room temperature for 7 hours, the solvent was evaporated, to afford 24.7 g of the title compound as a colorless oil.

출처