반응 #620762

ord-0bd0f8e4689c4c5b8364684eaad4b00f

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.ADDITIONan initial charge

실험 절차

Diethyl N-(3-trimethoxysilylpropyl)aminosuccinate was prepared as follows: 51.0 g of 3-aminopropyltrimethoxysilane (Silquest®A-1110, Momentive Performance Materials Inc., USA) were introduced as an initial charge. With thorough stirring, 49.0 g of diethyl maleate (Fluka Chemie GmbH, Switzerland) were added slowly at room temperature and the mixture was stirred at room temperature for 2 hours.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08853341B2uspto-grants-2014_10