반응 #619143
ord-a4ae14aff31d4e25a36f518125992004
반응 방정식
1,1-dicyclohexyl-3-(5-formyl-thiazol-2-yl)-urea
cyclopentylamine
sodium triacetoxyborohydride
→
desired product
수율 37.1%
1,1-Dicyclohexyl-3-(5-cyclopentylaminomethyl-thiazol-2-yl)-urea
수율 37.1%
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타Prepared
실험 절차
Prepared as described in general procedure (P) using 1,1-dicyclohexyl-3-(5-formyl-thiazol-2-yl)-urea (100 mg, 0.30 mmol), cyclopentylamine (45 μL, 0.45 mmol) and sodium triacetoxyborohydride (102 mg, 0.48 mmol) to afford 45 mg (37%) of the desired product after purification.