반응 #61221

ord-1e992dbb5630494eb2b5efd9f9b848c9

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타This compound was prepared

실험 절차

This compound was prepared using the general Sonagashira procedure as describe in General Procedures Example C, reacting N-(4-cyano-2-iodo-5-trifluoromethyl-phenyl)-methanesulfonamide (1.0 g, 2.56 mmol) and 1-ethylsulfanyl-2-methyl-but-3-yn-2-ol (0.37 g, 2.56 mmol) to yield the title compound as a yellow sticky oil.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07427682B2uspto-grants-2008_09