반응 #61214

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N-(2-iodo-4-nitro-5- trifluoromethyl-phenyl) -methanesulfonamide

3-(2,2,2-Trifluoro-ethylsulfanylmethyl) -pent-1yn-3-ol

→

title compound

2-(1-Methanesulfonyl-5-nitro-6-trifluoromethyl-1H-indol-2-yl)-1-(2,2,2-trifluoro-ethylsulfanyl)-butan-2-ol

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후처리

1. 1
   기타This compound was prepared

실험 절차

This compound was prepared using the general Sonagashira procedure as described in General Procedures Example C, reacting N-(2-iodo-4-nitro-5- trifluoromethyl-phenyl) -methanesulfonamide (0.62 g, 1.5 mmol) and 3-(2,2,2-Trifluoro-ethylsulfanylmethyl) -pent-1yn-3-ol (0.32 g, 1.5 mmol) to yield the title compound as a yellow sticky oil.

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