반응 #6100

반응 방정식

potassium hydroxide

2-hydroxybenzonitrile

dimethylthiocarbamoyl chloride

→

expected product

수율 94.0%

O-2-cyanophenyl dimethylthiocarbamate

수율 94.0%

반응 조건

실험 절차

If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.

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