반응 #6097

반응 방정식

potassium hydroxide

3-hydroxybenzonitrile

dimethylthiocarbamoyl chloride

→

expected product

O-3-cyanophenyl dimethylthiocarbamate

반응 조건

실험 절차

If the procedure described in Preparation XI is followed starting from 15 g (126.10-3 mol) of 3-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (132.10-3 mol) of potassium hydroxide, 29 g (quantitative yield) of the expected product are obtained.

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