반응 #60214

ord-c35c1b2444a44bd4a73c55c53dcc2698

반응 방정식

CN(C)CCN(CCNc1ccc([N+](=O)[O-])cn1)S(=O)(=O)c1ccccc1[N+](=O)[O-]
[2-(dimethylamino)ethyl]{2-[(5-nitro(2-pyridyl))amino]ethyl}[(2-nitrophenyl)sulfonyl]amine
OCCN1CCOCC1
4-(2-hydroxyethyl)morpholine
→
O=[N+]([O-])c1ccc(NCCN(CCN2CCOCC2)S(=O)(=O)c2ccccc2[N+](=O)[O-])nc1
(2-morpholin-4-ylethyl){2-[(5-nitro(2-pyridyl))amino]ethyl}[(2-nitrophenyl)sulfonyl]amine

반응물

CN(C)CCN(CCNc1ccc([N+](=O)[O-])cn1)S(=O)(=O)c1ccccc1[N+](=O)[O-]
[2-(dimethylamino)ethyl]{2-[(5-nitro(2-pyridyl))amino]ethyl}[(2-nitrophenyl)sulfonyl]amine
OCCN1CCOCC1
4-(2-hydroxyethyl)morpholine

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Made using the same procedure as for polymer-bound [2-(dimethylamino)ethyl]{2-[(5-nitro(2-pyridyl))amino]ethyl}[(2-nitrophenyl)sulfonyl]amine except that 4-(2-hydroxyethyl)morpholine (5.1 mL, 42 mmol) was used.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07425557B2uspto-grants-2008_09