반응 #6012
ord-e84ede7fe7a54153a4005eb838402408
반응 방정식
반응 조건
온도
45°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타the flask is fitted with a reflux condenser
실험 절차
9.9 ml (0.13 mol) of dimethylformamide are introduced dropwise and with stirring into a 250-ml flask containing 61.3 g (0.46 mol) of aluminum chloride, and the flask is fitted with a reflux condenser and heated in an oil bath to a temperature in the region of 45° C. 7.9 g (0.04 mol) of benzoselenazolinone and 10.6 g (0.06 mol) of nicotinoyl chloride hydrochloride are introduced.