반응 #600986

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N-(7-chloro-4-methoxy-quinolin-8-yl)-2-nitro-benzenesulfonamide

SnCl2

→

title compound

수율 92.3%

2-Amino-N-(7-chloro-4-methoxy-quinolin-8-yl)-benzenesulfonamide

수율 92.3%

용매

EtOH

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실험 절차

In a similar fashion using route 19 general procedure 29, N-(7-chloro-4-methoxy-quinolin-8-yl)-2-nitro-benzenesulfonamide 569 (580 mg, 1.4 mmol), SnCl2 (1.66 g, 7.3 mmol) in EtOH (20 ml) gave the title compound (470 mg, 92%) which was used in the next step without further purification.

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