반응 #599872

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2-bromo-5-iodo-1,3-dimethoxybenzene

thiophen-2-ylboronic acid

→

2-(4-Bromo-3,5-dimethoxyphenyl)thiophene

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후처리

1. 1
   기타Purification by chromatography (0-10% EtOAc-hexanes)

실험 절차

2-(4-Bromo-3,5-dimethoxyphenyl)thiophene was prepared from 2-bromo-5-iodo-1,3-dimethoxybenzene and thiophen-2-ylboronic acid according to the procedure used in Example 12. Purification by chromatography (0-10% EtOAc-hexanes) gave a yellow solid (0.624 g, 55% yield).

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