반응 #59928

반응 방정식

( 6f )

2-(((4-((2-methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

2-(2-(methoxymethyl)-1,3-dioxan-2-yl)ethanol

→

title compound

수율 7.0%

2-(((4-(2-(2-(methoxymethyl)-1,3-dioxan-2-yl)ethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

수율 7.0%

반응 조건

후처리

1. 1
   기타obtained in the step (36a)

실험 절차

The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using 2-(2-(methoxymethyl)-1,3-dioxan-2-yl)ethanol obtained in the step (36a) to obtain the title compound (304 mg, total yield: 7.0%) as a light yellow solid.

출처