반응 #59922

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( 6f )

2-(((4-((2-methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

(2-methyl-1,3-dioxan-2-yl)methanol

→

title compound

수율 8.6%

2-(((3-methyl-4-((2-methyl-1,3-dioxan-2-yl)methoxy)pyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

수율 8.6%

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후처리

1. 1
   기타obtained in the step (33a)

실험 절차

The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using (2-methyl-1,3-dioxan-2-yl)methanol obtained in the step (33a) to obtain the title compound (220 mg, total yield: 8.6%) as a light yellow solid.

출처