반응 #59918

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( 8g )

2-(((3-methyl-4-(2-(2-propyl-1,3-dioxan-2-yl)ethoxy)pyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

2-(2-methyl-1,3-dioxan-2-yl)ethanol

→

title compound

수율 2.5%

2-(((3-methyl-4-(2-(2-methyl-1,3-dioxan-2-yl)ethoxy)pyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

수율 2.5%

반응 조건

후처리

1. 1
   기타obtained in the step (30a)

실험 절차

The same procedure as in the steps (8c) to (8g) of Example 8, was repeated using 2-(2-methyl-1,3-dioxan-2-yl)ethanol obtained in the step (30a) to obtain the title compound (113 mg, total yield: 2.5%) as a light yellow solid.

출처