반응 #59908

반응 방정식

( 6f )

2-(((4-((2-methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

(2,2-diethyl-1,3-dioxan-5-yl)methanol

→

title compound

수율 9.7%

2-(((4-((2,2-diethyl-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1H-benzimidazole sodium salt

수율 9.7%

반응 조건

후처리

1. 1
   기타obtained in the step (23a)

실험 절차

The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using (2,2-diethyl-1,3-dioxan-5-yl)methanol obtained in the step (23a) to obtain the title compound (164 mg, total yield: 9.7%) as a light yellow solid.

출처