반응 #5983

ord-be42cc45ee0b43deb2da56f808879d43

반응 방정식

COC(=O)c1cc(Cl)c(NC(C)=O)c2c1OC1CCCCC21
methyl 1-acetylamino-2-chloro-5a,6,7,8,9,9a-hexahydrodibenzofuran-4-carboxylate
COC(=O)c1cc(Cl)c(NC(C)=O)c2c3c(oc12)CCCC3
methyl 1-acetylamino-2-chloro-6,7,8,9-tetrahydrodibenzofuran-4-carboxylate
COC(=O)c1cc(Cl)c(NC(C)=O)c2c1oc1ccccc12
methyl 1-acetylamino-2-chlorodibenzofuran-4-carboxylate
→
Nc1c(Cl)cc(C(=O)O)c2oc3ccccc3c12
1-AMINO-2-CHLORODIBENZOFURAN-4-CARBOXYLIC ACID

반응물

COC(=O)c1cc(Cl)c(NC(C)=O)c2c1OC1CCCCC21
methyl 1-acetylamino-2-chloro-5a,6,7,8,9,9a-hexahydrodibenzofuran-4-carboxylate
COC(=O)c1cc(Cl)c(NC(C)=O)c2c3c(oc12)CCCC3
methyl 1-acetylamino-2-chloro-6,7,8,9-tetrahydrodibenzofuran-4-carboxylate
COC(=O)c1cc(Cl)c(NC(C)=O)c2c1oc1ccccc12
methyl 1-acetylamino-2-chlorodibenzofuran-4-carboxylate

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타the captioned products are prepared

실험 절차

When the procedure of Example 15 is followed however methyl 1-acetylamino-2-chloro-5a,6,7,8,9,9a-hexahydrodibenzofuran-4-carboxylate is replaced by methyl 1-acetylamino-2-chloro-6,7,8,9-tetrahydrodibenzofuran-4-carboxylate or methyl 1-acetylamino-2-chlorodibenzofuran-4-carboxylate then the captioned products are prepared.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05246942uspto-grants-1993_09