반응 #595369

반응 방정식

methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate

→

title compound

methyl 4-hydroxy-2-isopropylbenzoate

용매

methanol

반응 조건

후처리

1. 1
   여과Then the mixture was filtered
2. 2
   농축the filtrate was concentrated

실험 절차

To a solution of methyl 4-(benzyloxy)-2-(prop-1-en-2-yl)benzoate (i-1d) (4.6 g, 16.3 mmol) in methanol (100 ml) was added Pd/C (0.46 g). The mixture was stirred at rt under H2 atmosphere for 24 h. Then the mixture was filtered, and the filtrate was concentrated to afford the title compound. LCMS (ESI) calc'd for C11H14O3 [M+H]+: 195.1. found: 195.1.

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