반응 #591

반응 방정식

CN1CC(c2ccccc2)Oc2nc

Cc1nccn1-c1ccc(N)cc1

→

Cc1nccn1-c1ccc(Nc2cc

수율 42.3%

용매

COCCOC

반응 조건

실험 절차

were placed in a microwave vial equipped with a stirring bar. The vial was capped and flushed with argon. DME (2 mL) was added via a syringe and the mixture was heated to 100°C in a microwave apparatus for 1h. The reaction mixture was filtered, the solvent was evaporated and the residue was purified by HPLC to give 53 mg (42 % yield) of the product as a solid.

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