반응 #59024
ord-4e49a290cc6449e9b2491cdda45e1841
반응 방정식
시약
없음
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타the solvent was evaporated under reduced pressure
- 2세척The residue was washed with water
실험 절차
Lithium hydroxide monohydrate (0.092 g) was added to a mixture of 4-ethoxycarbonyl-2-methoxyphenylboronic acid (0.049 g), water (1 mL) and 1,4-dioxane (1 mL), and the mixture was stirred at room temperature overnight. 2 mol/L hydrochloric acid (1.09 mL) was added to the reaction mixture, and the solvent was evaporated under reduced pressure. The residue was washed with water to afford the title compound (0.035 g).