반응 #58749

반응 방정식

5-bromo-pyridine-3-carbaldehyde

morpholine

→

title compound

수율 61.0%

4-(5-Bromo-pyridin-3-ylmethyl)-morpholine

수율 61.0%

반응 조건

후처리

1. 1
   기타The title compound was prepared in a similar way
2. 2
   기타The crude compound was purified (SiO2: 0-3% 2 M NH3 in MeOH/DCM)

실험 절차

The title compound was prepared in a similar way as described in Example 18, Step C, using 5-bromo-pyridine-3-carbaldehyde and morpholine. The crude compound was purified (SiO2: 0-3% 2 M NH3 in MeOH/DCM) to provide the title compound (61%).

출처